Unicorn, as the first single-mode microwave synthesizer of Bird & Bird, adopts the largest cylindrical single-mode resonance cavity with a volume of more than 500 ml, combined with Bottom-Feed rectangular waveguide bottom-feeding technology, which is targeted to solve the needs of small-dose experiments for precise control of microwave, especially suitable for organic synthesis, drug screening and research and development, fine nano-materials synthesis, macromolecule depolymerization, multiphase catalysis, and other fields. It is especially suitable for organic synthesis, drug screening and R&D, fine nanomaterials synthesis, polymer depolymerization, multiphase catalysis, etc.
| Microwave Source | Imported Toshiba |
|---|---|
| Power Supply | AC220V±10%，50HZ，10A |
| Microwave Frequency | 2450MHz |
| Microwave Input Power | 1500W |
| Microwave Output Power | 900W |
| Microwave power adjustment method | continuously adjustable |
| Material of Microwave Resonant Cavity | austenitic stainless steel |
| Microwave Resonant Cavity Volume | 500ml |
| Microwave Cavity Modes | single mode |
| Continuous Working Time | ≥72h |
| Primary Temperature Measurement Method | High Resolution Penetrating Fast Sensitive Response Infrared Sensor |
|---|---|
| Temperature Sensor Range | 50-350℃ |
| Maximum Operating Temperature | Atmospheric pressure 350°C, high pressure 250°C |
| Operating Temperature Control Range | 60-350℃ |
| Temperature Control Accuracy | ±1℃ |
| Response Speed | 5ms |
| Pressure Measurement Method | semiconductor piezoresistive effect |
|---|---|
| Pressure Sensor Range | 0-10MPa |
| Maximum Working Pressure | 5MPa |
| Working Pressure Control Range | 0-5MPa |
| Pressure Measurement Accuracy | 0.01MPa |
| Response Speed | 7ms |
| Norm | 0.5、5、10、30、100ml |
|---|---|
| Material | "Reaction bottle: quartz Seal cap: polytetrafluoroethylene (PTFE)" |
| Maximum withstand voltage | 5MPa |
| Frequency of use | Non-disposable, reusable |
| Rotary table station | |
|---|---|
| Temperature and pressure measurement and control system | |
| Whole Tank Temperature and Pressure Measurement System | |
| Full tank planetary magnetic stirring | |
| High Pressure Reaction Vessel Specification |
| Ultrasound source | |
|---|---|
| Ultrasonic frequency | |
| Ultrasonic power | |
| Ultrasonic power adjustment method | |
| Ultrasonic probe material | |
| Ultrasonic Probe Specifications | |
| Ultrasonic mode | |
| Ultrasonic high pressure reaction vessel |
| Fixed-position magnetic stirring | 1400r/min |
|---|---|
| Mechanical stirring | Support options |
| Digital Mechanical Stirring | Support options |
| Development Platform | Android-based |
|---|---|
| Screen | 10-inch color LCD touch screen |
| Processing Unit | Quad-core 1.2GHz |
| Random Access Memory | 2GB |
| Memory | 16GB |
| Real-time Monitoring System | 15 Megapixel HD Camera 5 Megapixel HD Camera |
| USB interface | support sth. |
| Temperature-Pressure Coordinated Control | Temperature/pressure dual measurement and control system, real-time monitoring of temperature/pressure changes in the reaction system, up to the set value of the instrument automatically control temperature and pressure. |
| Microwave-Ultrasonic Synergistic Control | / |
| Cooling System | Eddy current cooling (standard) + air compressor (optional) |
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| Wavelength | |
|---|---|
| Power | |
| Reaction Vessel Material | |
| Light Intensity Detection |
| Pre-Injection Booster System | Before the start of the reaction, the atmosphere in the quartz high-pressure closed reactor can be adjusted for gas injection, pumping and gas exchange experiments. |
|---|---|
| Solid Phase Reaction Apparatus | Upgraded the original infrared sensor to a larger range sensor of the same type, penetrating the quartz vessel wall to directly measure the temperature of the reactants, equipped with a special crucible for pure solid-phase reactions in a microwave environment and thermal insulation structure. |
| Photocatalytic Module | High and medium power density wavelengths can be selected, equipped with microwave environment-specific quartz fiber, to achieve microwave radiation and in situ light synergistic reaction |
| Microwave Radiation Synchronized Cooling | Customized modification of waveguide cut-off top cover, additional water inlet and outlet, good microwave shielding. Equipped with jacketed flasks, which can take away the heat by external refrigerant during microwave heating to maximize the microwave output power. |
| Helical Tube Flow Reactor | / |
| ID | Organization/Institution/Company | Sector | Purchase date |
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